1.

Discuss briefly de-mineralisation of water by ion exchange resin.

Answer»

Solution :SYNTHETIC resins method : Nowadays hard water is softened by using synthetic cation exchangers. This method is more efficient than zeolite process.
Cation exchange resins : It contain large organic molecule with -`SO_3H` group and are water insoluble. Ion exchange resin `(RSO_3H)` is changed to RNa by treating it with NaCl.
The resin exchanges `Na^+` ions with `Ca^(2+)` and `Mg^(2+)` ions present in hard water to make the water soft. Here R is resin anion.
`2RNa_((s)) + M_((aq))^(2+) to R_2M_((s)) + 2Na_((aq))^(+)`
The resin can be regenerated by adding aqueous NaCl solution.
Pure de-mineralised (de-ionized) water free from all soluble mineral salts is obtained by passing water successively through a cation exchange in the `H^+` form) and an anion exchange in the `OH^-` form) resins.
`2RH_((s)) + M_((aq))^(2+) hArr MR_(2(s)) + 2H_((aq))^(+)`
In this cation exchange process, `H^+` exchanges for `Na^(+) , Ca^(2+), Mg^(2+)` and other cations present in water.
This process results in proton release and thus makes the water acidic.
Anion exchange process :
`RNH_(2(s)) + H_2O_((l)) hArr RNH_(3)^(+) . OH_((s))^(-)`
`RNH_3^(+) . OH_((s))^(-) + X_((aq))^(-) hArr RNH_3^(+) . X_((s))^(-) + OH_((aq))^(-)`
`OH^-` exchanges for ANIONS like `Cl^(-), HCO_3^(-) , SO_4^(2-)` etc. present in water . `OH^-` ions, thus, liberated neutralise the `H^+` ions set free in the cation exchange.
`H_((aq))^(+)+ OH_((aq))^(-) to H_2O_((l))`
The exhausted cation and anion exchange resin beds are regenerated by treatment with DILUTE acid and alkali solutions respectively.


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