1.

Write the principles of the following methods: (i) Vapour phase refining (ii) Zone refining (iii) Chromatography

Answer» (i) Vapour phase refining: In this method, crude metal is freed from impurities by first converting it into a suitable volatile compound by heating it with a specific reagent at lower temperature and then decomposing the volatile compound at some higher temperature to given the pure metal.
(ii) Zone refining: It is based upon the principle that the impurities are more soluble in the molten state than in the solid state of the metal.
(iii) Chromatography: It is based upon the principle that the different components of a mixture are adsorbed to different extents on an dsorbent


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